• 专利附录
  • 专利说明
  • 权利要求
  • 类似技术
  • 同族专利
  • 引用文献
  • 法律状态
  • 优先权
    • 专利摘要:
    Label, system and method for the detection of long-distance objects. The present invention describes a label comprising a magnetic element in the form of a microwire of 80-250 microns with a giant magnetoimpedance that, when attached to an object, allows its wireless detection by modulating the micrail's reflectivity. The detection is performed using a system that emits an electromagnetic wave of frequency between 1 and 20 ghz and a magnetic field of low frequency (0.01 - 50 hz) and detects the modulation of the reflectivity of the microwire. In this way, objects are detected at distances greater than 1 m. (Machine-translation by Google Translate, not legally binding)
    公开号:ES2581127A1
    申请号:ES201600298
    申请日:2016-04-13
    公开日:2016-08-31
    发明作者:María Pilar MARÍN PALACIOS；Antonio Hernando Grande
    申请人:Universidad Complutense de Madrid；
    IPC主号:
    专利说明:

    Label, system and method for long-distance object detection. Technical sector
    The present invention falls within the field of object detection through electromagnetic fields. More specifically, the invention relates to a wireless long-distance detectable label formed by an active element and a complementary element, both magnetic, as well as to the system and method of object detection using said label. State of the art
    The present invention relates to a system for the electronic detection of long-distance objects based on the influence of magnetic phenomena on the reflectivity of GHz waves encompassing. in particular, the labels that can be activated / deactivated and their system and method of detection.
    Systems for the detection of articulations based on magnetic materials are well known. The FR763681 patent shows the first device of this type. The described device is based on the use of a tape of soft magnetic material of the Permalloy type that subjected to an alternating magnetic field induces harmonics in a detector clearly different from those from another type of metals
    The amorphous magnetic materials in the form of tape have low coercive fields and high susceptibility that can be optimized to be used in equipment for the electronic detection of articles by means of suitable heat treatments in the presence or not of the magnetic field. WO0213210 refers to the use of compositions based on CoNiFeSiBC.
    In US4660025 a detector system is shown in which a bistable magnetic amorphous thread of minimum length 7.6 cm is used as a label. In this case an alternating magnetic field is applied to a certain region of space and an alarm is activated when a disturbance of said magnetic field is detected. This occurs when the label is introduced in that region and the value of the magnetic field exceeds the critical field of the wire causing the magnetization to reverse. This is known as snap action. A drawback of these systems is the high tag length.
    In addition to the advantages obtained in the US4660025 patent label and which refer to its high harmonic content and high pulse, it is important to find the possibility of deactivating this type of magnetic materials. US4686516 shows a way of doing it from the crystallization of amorphous magnetic material. This is done by heating, at least a part of the label, above its crystallization temperature either by applying an electric current or a radiant energy like a laser. Although some of the procedures presented here allow you to deactivate the label without touching it, they need to be carefully applied.
    The US4980670 patent shows a magnetic marker for electronic monitoring of articles where the tag has "snap action" for low threshold values of the applied magnetic field and also the tag is easily deactivatable.
    US5313192 develops a label equivalent to that described in US4980670 but more stable and controllable. The processing conditions of the amorphous magnetic tape are the same but, in addition, the label is subjected to predetermined magnetic fields during processing that allow it to be activated and deactivated. More particularly, the tag of this invention contains a soft magnetic material that constitutes the main core and a second hard or semi-hard magnetic material. This label is conditioned in such a way that the second material has states activated and deactivated respectively. In the activated state the tag exhibits bistable hysteresis while in the deactivated the tag it presents a hysteresis cycle without Brakhausen hops.
    US6747559 refers to a permanent label for electronic detection of articles based on magnetic micro-wires with low coercive field (less than 10 A / m) and high magnetic permeability (greater than 20,000). The length of the thread
    or used threads is not more than 32 mm. In this case, it is the high permeability that makes it possible to obtain high order harmonics and with great amplitude for sufficiently low applied field values, thus making the label easy to distinguish.
    US7852215 has a magnetic microwire based tag for operating according to the induction method in a manner equivalent to that described in US6747559.
    All the systems described are based on harmonic generation and have a clear limitation in the detection distance limiting it to about 90 cm. Another limitation is the difficulty in detecting signals from other types of metals.
    There are systems that allow detection at a greater distance, never exceeding two meters, based on magnetoelastic resonance such as the one claimed in US4510489. It uses magnetomechanical labels based on magnetostrictive elements that oscillate in the presence of an alternating magnetic field of the mechanical resonance frequency. An equivalent system but using magnetoelastic micro wires is the one presented in the patent ES2317769 (B1).
    Another limitation of these systems is the size of the label to use.
    Patent US6232879 bases the remote detection of objects on a label formed by at least two elements in a certain relative position which limits the size and geometry of the label.
    Therefore, there is a need to develop small-sized and easily detectable labels over longer distances. Detailed description of the invention
    Label, system and method for long-distance object detection.
    The present patent presents the possibility of a magnetic micro wire as a sensor element of small length detectable at high distances (greater than 1 meter) whose detectability is conditioned by the relationship between its coercive field and frequency.
    The invention relates to a label formed by an active element and, optionally, a complementary element, both magnetic, which allows its long-distance detection wirelessly by modulating the reflectivity of the active element.
    The active element is a soft magnetic wire of diameter between 80 and 200 microns, with giant magnetoimpedance and length conditioned by the emission frequency of the antennas so that, for excitation frequencies between 1 and 20 GHz the length of the element to be detected It is between 30 and 1 cm; more precisely, for a frequency of 3 GHz a 5 cm sensor element would be used and for 1.5 GHz, 10 cm.
    The coercive field shown by the micro thread depends on the frequency of this low frequency field. Said magnetic wire must have a non-bistable hysteresis cycle with transverse anisotropy between 10 and 20 Oe and its coercive field, between 1 and 5 Oe, for frequencies of a low frequency exciter field between 10 and 50,000 m Hz, never higher.
    The micro thread can be both an elongated and closed micro thread, for example, in the form of a ring, square or rectangle, with one or more turns or in the form of micro-wire powder.
    In more detail, the active element is a magnetic micro-wire with borosilicate glass cover of iron and cobalt-based composition, for example, FexCoa-x-yNiySizBwMt (where a + z + w + t = 100, 70≤axy≤75 , 0≤x + y≤5, 0≤z + w≤25, 0≤t≤3, M = Nb, Mo, Hf) with a virtually zero magnetostriction constant whose values are between -1 ppm and -0, 05 ppm, with anisotropy field not less than 10 Oe and not more than 20 Oe and with a metal core diameter of between 30 and 250 microns. Its composition can be amorphous or nanocrystalline with a coercive field between 0.5 and 250 Oe (for frequencies of the low frequency exciter field of 0.001 and 50 Hz, never higher) with property of giant magnetoimpedance, with proper thread geometry, ring, coil , rectangular circuit or magnetic micro-wire powder, where the frequency of electrical resonance of these geometries is conditioned by their geometric parameters in the frequency range between 1 and 20 GHz.
    The dimensions of the thread are between 30 and 1 cm, the diameter of the ring between 0.5 and 10 cm, the side of the rectangle between 0.5 and 10 cm or the length of the powder micro threads between 1 and 5 mm.
    The magnetic permeability, due to the low magnetic anisotropy of the micro thread, is easily modifiable by applying a magnetic field.
    In addition, the coercive field of the thread of the active element increases when the frequency of the low frequency field increases and the maximum variation in the reflectivity of the active element occurs for low frequency fields associated with coercive fields of the active element between 1 and 20 Hz.
    The coercive field of the active element is controlled through the composition of the wire and nano-crystallization thermal treatments.
    The magnetoimpedance effect between 20 and 50% is controllable through the percentage of nanocrystallization between 0 and 10%.
    The second element (complementary element) may be a magnetic wire with a diameter greater than 100 microns or a magnetic tape or a magnetic powder, the remanence of which is such that. in the vicinity of the soft magnetic wire, create a magnetic field in the order of its coercive field at the frequency of the exciter field.
    The presence of this second magnetic element with magnetization such that it generates a magnetic field in the vicinity of the micro wire equivalent to its coercive field maximizes the reflectivity of the micro wire.
    In addition, this second element can also be used as a label deactivator because, once used, its magnetization state could be modified by applying an intense magnetic field and leaving the label deactivated.
    Another aspect of the invention relates to a long distance object detection system by wireless detection of the micro thread described above. The detection system consists of a transmitter system connected to a transmitter antenna and a receiver system connected to a receiver antenna. The emitting antenna emits a fixed frequency wave between 0.5 and 6 GHz. A wave polarizer is used in one direction or rotary to make sure that the electric field of the wave is in the axial direction of the element to be detected and a system Low frequency signal generator, between 10 and 50,000 m Hz (never higher), connected to coils for the creation of a magnetic field of low frequency alternating modulation to which, optionally, a continuous field in the area of detection. All this is controlled by a controller system connected to the transmitter device, the receiver and the low frequency signal generator. The receiver system collects the variations in the reflectivity of the element to be detected, modulated by the superposition of the continuous and low frequency magnetic fields, respectively.
    The detection system comprises a first electrical circuit fed by a low frequency sinusoidal signal to which another continuous electric current (DC) can be superimposed that feeds a winding, camouflaged on the ground, which generates a magnetic field lower than the anisotropy field of the used thread. Said circuit allows the magnetization and periodic demagnetization of the soft magnetic thread placed on the label. The system comprises a second circuit that is used to emit and receive, by means of both transmitting and receiving antennas, a high frequency signal such that the frequency coincides with the electrical resonance frequency of the chosen thread. In addition, the system comprises means for processing the signal by establishing a detection threshold.
    A third aspect of the invention relates to the method of detecting long-distance objects using the label described. It is based on the modulation, by the magnetic micro wire, of the wave emitted by the emitting antenna. This modulation is due to the variations experienced by the reflective coefficient of the micro thread in the presence of an alternating magnetic field of low frequency and is maximum when there is the greatest variation in the permeability of the thread that coincides with its coercive field.
    For this specific case, the electromagnetic wave dispersion coefficients, due to the magnetic susceptibility, are simultaneously modified by:
    - the frequency of the alternating magnetic field generated by the electrical circuit (that is, the first circuit of the detection system) and involves the periodic magnetization of the
    micro thread, with a frequency between 0.01 and 50 Hz, the optimum frequencies for detection always being lower than a certain value that is conditioned by the microstructure of the wire. In the case of amorphous microstructure the optimal frequencies would be less than 10Hz and in the case of crystalline microstructure, 20 Hz.
    - the amplitude of the alternating magnetic field generated by the electrical circuit (that is, the first circuit of the detection system) and involves the periodic magnetization of the micro wire, with a frequency between 0.01 and 50 Hz, with the optimal amplitudes for detection being lower to the anisotropy fields of the wires and between the middle of the anisotropy field and the anisotropy field itself.
    The detection of the tag is done by modulating the reflectivity of its active element (the micro wire) with respect to electromagnetic waves of frequency between 1 and 20 GHz used, for this, a low frequency magnetic field that can be between 0.01 and 50 Hz. The amplitude of the field is between 0 and 25 Oe.
    The modulation of the micro wire's reflectivity is done with the frequency of this low frequency field and is a consequence of the giant magnetoimpedance effect experienced by the active element.
    In addition, the maximum variation in the reflectivity of the active element occurs for its electrical resonance frequencies conditioned by the geometry (length in the case of a wire, diameter in the case of ring and side lengths in the case of square or rectangle) .
    This modulation of the reflectivity of the active element implies the modulation of the GHz wave in the presence of said element and its detection is done by means of an antenna through the wave modulated in GHz in the presence of a magnetic active element subjected to a low field frequency.
    The generation of the magnetic field is of low frequency can be done, for example, by means of rectangular coils camouflaged on the ground and the generation and detection of GHz waves can be performed by a system of camouflaged antennas on the ceiling. Brief description of the figures
    Figure 1 shows schemes corresponding to different label configurations: wire (1) with soft magnetic wire (1 ') and (11'), ring (2), (2 ') and (2 "), square (3), (3 ') and (3 ") and micro thread powder (4).
    Figure 2 shows a scheme of the electromagnetic circuit with the following elements: label with micro thread (5), emitting antenna (6), receiving antenna (7), emitted wave (8), modulated wave (9), low field coil frequency (10), function generator (11), amplifier (12), ammeter (13) and vector analyzer (14).
    Figure 3 shows the hysteresis cycles, obtained by the 10 Hz induction method, associated with two 10 and 15 cm micro wires with the required parameters of anisotropy field with values, in this case, of 17 Oe (15) and 22 Oe (16), respectively. and of coefficient coefficient of 1 Oe (17).
    Figure 4 shows the hysteresis cycles corresponding to a 15 cm wire at different frequencies: 10Hz (18), 20Hz (19), 30Hz (20), 40Hz (21) and 50Hz (22).
    Figure 5 shows the evolution of the coercive field with the frequency for a 15 cm thread.
    Figure 6 shows the reflectivity as a function of the time detected by the antenna (6) and associated with the modulated wave (9) with the frequency of the low frequency field for a wave frequency emitted by the antenna of 2.37 GHz and a field applied low frequency of 2.5 Oe.
    Figure 7 shows the evolution of the maximum reflectivity as a function of the frequency of the low frequency field of 2.5 Oe for the 2.37 GHz wave.
    Figure 8 shows the evolution of the maximum reflectivity for frequencies between 10 and 50 Hz when a continuous magnetic field is applied.
    Figure 9 shows the maximum reflectivity as a function of time for two micro threads, one soft and the other hard: with the thread desimanado (a) and saturated (b). Embodiment of the invention
    The present invention is further illustrated by the following example that is not limiting of its scope.
    A label consisting of two parallel threads of 15 cm in length and FeCoSiB composition is selected having one of the amorphous structure threads and the other crystalline structure threads. Their hysteresis cycles are performed at different frequencies to determine their coercive field as a function of frequency (Figure 3).
    The transmitting and receiving antennas are connected to a vector analyzer working at a frequency of 2.37 GHz. By means of coils a low frequency magnetic field is generated between 10 and 50 Hz of maximum amplitude 2.5 Oe. The evolution of the reflectivity as a function of time according to the frequency of the low frequency field (Figure 9) and the evolution of the reflectivity with the value of the DC field superimposed to that of low frequency (Figure 8) is measured ) and, for the hard wire magnetized reflectivity as a function of frequency (Figure 9).
    The detection of the micro thread is made from the amplitude of the detected signal and its variation with respect to that observed in the absence thereof. The amplitude of the signal is greater the lower the frequency of the low frequency field. In the presence of a magnetically hard wire it is possible to decrease the voltage of this signal which would result in deactivation of the tag.
    权利要求:
    Claims (21)
    [1]
    one.  Label comprising a magnetically soft micro wire (active element) with a diameter between 80 and 250 microns, with giant magnetoimpedance property, with non-bistable hysteresis cycle with transverse anisotropy between 10 and 20 Oe, coefficient field between 1 and 5 Oe for a low frequency exciter field between 10 and 50,000 mHz and amplitude between 0 and 25 Oe and whose high frequency electric resonance frequency is conditioned by its geometric parameters for excitation frequencies between 1 and 20 GHz.
    [2]
    2.  Label, according to claim 1, which preferably comprises another magnetically hard element in the form of a wire with a diameter greater than 100 microns or a magnetic tape or a magnetic powder whose remanence is such that in the vicinity of the magnetically soft micro thread creates a magnetic field of the order of its coercive field at the frequency of an exciter field.
    [3]
    3.  Label according to claim 2, wherein the hard magnetic element acts as a deactivator of the label because, once used, its magnetization state could be modified by applying an intense magnetic field and leaving the label deactivated.
    [4]
    Four.  Label, according to previous claims, wherein the micro thread can be both an elongated and closed micro thread, for example, in the form of a ring, square or rectangle, with one or more turns.
    [5]
    5.  Label according to claim 4, wherein the dimensions of the micro thread are between 30 and 1 cm, the diameter of the ring between 0.5 and 10 cm, the side of the rectangle between 0.5 and 10 cm or the length of the powder micro threads between 1 and 5 mm.
    [6]
    6.  Label, according to previous claims, wherein the length of the micro thread is 5 cm for a frequency of 3 GHz and 10 cm for a frequency of 1.5 GHz.
    [7]
    7.  Label, according to previous claims, where the micro-wire coefficient field increases with increasing frequency of the low frequency exciter field and the maximum variation of the reflectivity occurs for low frequency fields associated with micro-wire coefficient fields between 1 and 20 Hz.
    [8]
    8.  Label according to claim 1, wherein the composition of the micro thread is based on iron and cobalt with amorphous or crystalline structure.
    [9]
    9.  Label according to claim 8, wherein the micro thread has FexCOax-yNiySizBwMt composition (where a + z + w + t = 100, 70≤axy≤75, 0≤x + y≤5, 0≤z + w≤25, 0≤ t≤3, M = Nb, Mo, Hf).
    [10]
    10. Label, according to claims 8 and 9, wherein the magnetoimpedance of the micro thread between 20 and 50% is controlled through its percentage of nanocrystallization, between 0 and 10%.
    [11]
    eleven.  Label according to claims 8 to 10, wherein the micro thread has a virtually zero magnetostriction constant whose values are between -1 ppm and -0.05 ppm, with anisotropy field not less than 10 Oe and not more than 20 Oe, with a metal core diameter of value between 30 and 250 microns and a field
    coercive between 0.5 and 250 Oe (for frequencies of a low frequency exciter field of 0.01 and 50 Hz) and electrical resonance frequency of these geometries is conditioned by their geometric parameters in the frequency range between 1 and 20 GHz
    [12]
    12.  Use of the claimed label for object detection.
    [13]
    13.  Use according to claim 12 for the detection of objects at a distance greater than 2 meters.
    [14]
    14.  System for the detection of long-distance objects where the object has the claimed label and which comprises:
    - A transmitter system connected to a transmitter antenna that emits a frequency wave between 1 and 20 GHz.
    - A generator system low frequency signal generator system, between 10 and 50,000 mHz for the creation of a magnetic field of alternating modulation of low frequency to which a continuous field is superimposed in the detection zone.
    - A receiver system that collects the variations in the micro-thread reflectivity of the tag, modulated by the superposition of the continuous and low frequency magnetic fields, respectively.
    - A controller system connected to the transmitter device, the receiver and the low frequency signal generator.
    [15]
    fifteen.  Detection system. according to claim 14, comprising a first electrical circuit fed by a low frequency sinusoidal signal to which it is superimposed on another direct electric current (DC) that feeds a winding, camouflaged on the ground, which generates a magnetic field below the field of anisotropy of the used thread. Said circuit allows the magnetization and periodic demagnetization of the soft magnetic thread placed on the label. The system comprises a second circuit for emitting and receiving, by means of both transmitting and receiving antennas, a high frequency signal such that the frequency coincides with the electrical resonance frequency of the chosen thread. In addition, the system comprises means for processing the signal by establishing a detection threshold.
    [16]
    16.  Detection system according to claims 14 and 15, wherein the frequency of the low frequency magnetic field to be used is determined by the evolution with the frequency of the magnetic micro-wire coercive field to be detected.
    [17]
    17.  Detection system according to claims 14 to 16, wherein the generation of the low frequency magnetic field is done by camouflaged coils on the ground.
    [18]
    18. Detection system according to claims 14 to 16, wherein the generation and detection of waves is carried out by means of a system of camouflaged antennas on the ground.
    [19]
    19.  Method for long-distance detection of objects using the claimed system whose detection is performed by modulating the reflectivity of the micro thread by
    the superposition of the continuous and low frequency magnetic fields comprising:
    - Emit an electromagnetic wave of frequency between 1 and 20 GHz
    - Create an alternating magnetic field of low frequency, which has a frequency between 10 and 5000 m Hz and an amplitude between 0 and 25 Oe.
    - Superimpose an electric current to the alternating low-frequency magnetic field
    10 continuous (DC) that generates a magnetic field lower than the anisotropy field of the used thread.
    - Measure the evolution of the reflectivity of the thread based on the time and frequency of the low frequency field.
    [20]
    20. A method according to claim 19, wherein the modulation of the micro-wire reflectivity involves modulating the GHz wave in the presence of said micro-wire and its detection is performed by an antenna through the GHz-modulated wave in the presence of a Magnetic active element subjected to a low frequency field.
    [21]
    21. Method according to claim 19, wherein the maximum detection occurs for the lowest possible frequency of the low frequency field.
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